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Synthesis and characterization of 1,6‐and 1,7‐dihydroxy alkanes and their acrylic esters. I
Author(s) -
Shantha K. L.,
Pratap G.,
Rao V. S. Bhaskar,
Krishnamurti N.
Publication year - 1990
Publication title -
journal of applied polymer science
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.575
H-Index - 166
eISSN - 1097-4628
pISSN - 0021-8995
DOI - 10.1002/app.1990.070410506
Subject(s) - aluminum hydride , acrylic acid , lithium (medication) , chemistry , infrared , polymer chemistry , nuclear chemistry , characterization (materials science) , materials science , organic chemistry , ion , copolymer , polymer , medicine , physics , optics , nanotechnology , endocrinology , methoxide
The 1,6‐ and 1,7‐dihydroxy alkanes having chain lengths C 13 –C 24 were synthesized in high purity by lithium aluminum hydride reduction of corresponding 6‐oxo and 7‐oxoalkanoic acids. These were then converted to 6‐hydroxy and 7‐hydroxy acrylic esters, respectively, and were characterized by infrared, 1 H nuclear magnetic resonance, and mass spectroscopic methods.