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A facile one‐pot synthesis of [(COD)Pt(CH 3 ) 2 ]
Author(s) -
Wen Fei,
Bönnemann Helmut
Publication year - 2005
Publication title -
applied organometallic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.53
H-Index - 71
eISSN - 1099-0739
pISSN - 0268-2605
DOI - 10.1002/aoc.842
Subject(s) - chemistry , cyclooctadiene , platinum , yield (engineering) , 1,5 cyclooctadiene , elemental analysis , mass spectrometry , carbon 13 nmr , organic chemistry , nuclear chemistry , catalysis , chromatography , metallurgy , materials science
A novel one‐pot synthesis of dimethyl(1,5‐cyclooctadiene)platinum(II), i.e. [(COD)Pt(CH 3 ) 2 ] (complex 1), was developed in 92% yield using platinum acetylacetonate, 1,5‐cyclooctadiene and trimethylaluminium. Complex 1 was fully characterized by 1 H and 13 C NMR, mass spectrometry, cell dimensions and elemental analysis. Copyright © 2005 John Wiley & Sons, Ltd.
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