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2‐HC 12 CI 9 : A simple synthesis of PCB‐206
Author(s) -
Humphries R E,
Massey A G
Publication year - 1993
Publication title -
applied organometallic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.53
H-Index - 71
eISSN - 1099-0739
pISSN - 0268-2605
DOI - 10.1002/aoc.590070211
Subject(s) - chemistry , simple (philosophy) , stereochemistry , medicinal chemistry , epistemology , philosophy
A one‐pot synthesis is described for polychlorobi‐phenyl number 206. Addition of C 6 Cl 5 Li to tetrachlorobenzyne gives 2‐LiC 12 Cl 9 , which undergoes Li/H exchange with C 6 Cl 5 H to form 2, 2′, 3, 3′, 4, 4′, 5, 5′, 6‐nonachlorobiphenyl