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Preparation of core/shell/shell CoFe 2 O 4 /OCMC/Cu (BDC) nanostructure as a magnetically heterogeneous catalyst for the synthesis of substituted xanthenes, quinazolines and acridines under ultrasonic irradiation
Author(s) -
Ghasemzadeh Mohammad Ali,
Ghaffarian Fatemeh
Publication year - 2020
Publication title -
applied organometallic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.53
H-Index - 71
eISSN - 1099-0739
pISSN - 0268-2605
DOI - 10.1002/aoc.5580
Subject(s) - chemistry , catalysis , scanning electron microscope , nanocomposite , nuclear chemistry , nanostructure , adsorption , heterogeneous catalysis , desorption , chemical engineering , fourier transform infrared spectroscopy , organic chemistry , materials science , composite material , engineering
Highly efficient synthesized magnetic cobalt ferrite nanoparticles supported on OCMC@Cu (BDC) was utilized in the preparation of biologically active heterocyclic compounds through one‐pot three‐component reactions between of aldehydes, dimedone, aryl amines/2‐naphthol/urea under ultrasonic irradiation. This method has various advantages including excellent yields, little catalyst loading, simple procedure, facile catalyst separation, short reaction times, eco‐friendly approach and simple purification. The catalyst was characterized by various spectroscopy methods such as fourier‐transform infrared (FT‐IR), energy‐dispersive X‐ray (EDX), scanning electron microscope (SEM), X‐ray diffraction (XRD) and N 2 adsorption–desorption isotherm (BET). Furthermore, the heterocyclic compounds were characterized by spectral techniques. The nanocomposite was simply separated byusing an external magnet, and it can be recycled several times without significant loss of activity.