Facile preparation of highly stable and active hybrid palladium nanoparticles: effectual, reusable and heterogeneous catalyst for  coupling reactions | Zendy

Adib Mehdi | Zendy; Yasaei Zahra | Zendy; KarimiNami Rahman | Zendy; Khakyzadeh Vahid | Zendy; Veisi Hojat | Zendy

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Facile preparation of highly stable and active hybrid palladium nanoparticles: effectual, reusable and heterogeneous catalyst for coupling reactions

Author(s) -

Adib Mehdi,

Yasaei Zahra,

KarimiNami Rahman,

Khakyzadeh Vahid,

Veisi Hojat

Publication year - 2016

Publication title -

applied organometallic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.53

H-Index - 71

eISSN - 1099-0739

pISSN - 0268-2605

DOI - 10.1002/aoc.3499

Subject(s) - sonogashira coupling , chemistry , catalysis , palladium , coupling reaction , aryl , inductively coupled plasma , nanoparticle , inductively coupled plasma atomic emission spectroscopy , solvent , heterogeneous catalysis , fourier transform infrared spectroscopy , transmission electron microscopy , combinatorial chemistry , nuclear chemistry , inorganic chemistry , chemical engineering , organic chemistry , plasma , quantum mechanics , alkyl , physics , engineering

Palladium nanoparticles were supported on a bed of Fe 3 O 4 @‐NH 2 @Murexide using a simple and efficient method, and characterized using Fourier transform infrared spectroscopy , X‐ray diffraction, scanning and transmission electron microscopies and inductively coupled plasma optical emission spectrometry . The catalytic system showed great efficiency in cross‐coupling reaction of aryl iodides and arylboronic acid and in Sonogashira cross‐coupling reaction in the green solvent EtOH–H 2 O (1:1). The isolation and recovery of the catalyst were simple and facile and it could be used for several successive Suzuki–Miyaura coupling and Sonogashira cross‐coupling reactions . Copyright © 2016 John Wiley & Sons, Ltd.

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