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Eco‐friendly synthesis of benzoxazepine and malonamide derivatives in aqueous media
Author(s) -
Babazadeh Mirzaagha,
HosseinzadehKhanmiri Rahim,
Zakhireh Solmaz
Publication year - 2016
Publication title -
applied organometallic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.53
H-Index - 71
eISSN - 1099-0739
pISSN - 0268-2605
DOI - 10.1002/aoc.3463
Subject(s) - chemistry , aqueous medium , aqueous solution , catalysis , environmentally friendly , organic chemistry , infrared , carbon 13 nmr , infrared spectroscopy , nuclear chemistry , combinatorial chemistry , ecology , physics , optics , biology
A special, efficient and reusable heterogeneous catalytic system is reported for the one‐pot three‐component synthesis of a series of malonamide and 2,3,4,5‐tetrahydrobenzo[ b ][1,4]oxazepine derivatives in the presence of a heterogeneous material composed of MCM‐48/H 5 PW 10 V 2 O 40 in aqueous media and at room temperature. The products were identified using physical data (melting points) by comparison with those reported in the literature. Also, the structures of the new compounds were characterized by means of infrared, 1 H NMR, 13 C NMR and CHN analyses. Copyright © 2016 John Wiley & Sons, Ltd.