Synthesis and characterization of Pd(II) complexes of 2‐ and 3‐thiophenecarbaldehyde immobilized on silica obtained from sepiolite | Zendy

Corral Jorge | Zendy; Mora Manuel | Zendy; JiménezSanchidrián César | Zendy; Ruiz José Rafael | Zendy

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Synthesis and characterization of Pd(II) complexes of 2‐ and 3‐thiophenecarbaldehyde immobilized on silica obtained from sepiolite

Author(s) -

Corral Jorge,

Mora Manuel,

JiménezSanchidrián César,

Ruiz José Rafael

Publication year - 2013

Publication title -

applied organometallic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.53

H-Index - 71

eISSN - 1099-0739

pISSN - 0268-2605

DOI - 10.1002/aoc.3028

Subject(s) - chemistry , sepiolite , bromobenzene , phenylboronic acid , palladium , catalysis , nuclear chemistry , polymer chemistry , mesoporous silica , organic chemistry , inorganic chemistry , mesoporous material , raw material

Silica obtained by acid treatment of sepiolite was used as a support for catalysts consisting of palladium complexes of 2‐ and 3‐thiophenecarbaldehyde. The support and the catalysts were characterized by X‐ray diffraction, and solid‐state 29 Si and 13 C nuclear magnetic resonance spectroscopies. The supported palladium catalysts were used in the Suzuki reaction of bromobenzene with phenylboronic acid. Copyright © 2013 John Wiley & Sons, Ltd.

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