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New steroid‐group‐containing borazine compounds and their 13 C NMR spectra
Author(s) -
Yamashita Hiroshi,
Koda Naoko,
Murakami Teiichi,
Uchimaru Yuko
Publication year - 2002
Publication title -
applied organometallic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.53
H-Index - 71
eISSN - 1099-0739
pISSN - 0268-2605
DOI - 10.1002/aoc.265
Subject(s) - chemistry , borazine , steroid , nmr spectra database , group (periodic table) , stereochemistry , organic chemistry , medicinal chemistry , spectral line , biochemistry , physics , astronomy , boron nitride , hormone
New borazine compounds containing steroid units (cholesteryl and stigmasteryl) were prepared by the reactions of B,B ′, B ″‐trichloro‐ N,N ′, N ″‐trimethylborazine with the 3‐chloro derivatives of the corresponding steroids under Grignard conditions. The products were characterized by 13 C– 1 H correlation NMR measurements to give fully assigned 13 C NMR data. Copyright © 2001 John Wiley & Sons, Ltd.