Syntheses and structures of Me 3 Sb + CH 2 COO − ·H 2 O, the monohydrate of the antimony analogue of betaine, and related compounds | Zendy

Balàzs Gàbor | Zendy; Balàzs Lucia | Zendy; Breunig Hans J. | Zendy; Lork Enno | Zendy

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Syntheses and structures of Me 3 Sb + CH 2 COO − ·H 2 O, the monohydrate of the antimony analogue of betaine, and related compounds

Author(s) -

Balàzs Gàbor,

Balàzs Lucia,

Breunig Hans J.,

Lork Enno

Publication year - 2002

Publication title -

applied organometallic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.53

H-Index - 71

eISSN - 1099-0739

pISSN - 0268-2605

DOI - 10.1002/aoc.255

Subject(s) - chemistry , antimony , betaine , crystal structure , x ray crystallography , single crystal , crystallography , stereochemistry , inorganic chemistry , organic chemistry , diffraction , physics , optics

The syntheses of the antimony analogue of betaine, Me 3 Sb + CH 2 COO − (1), of the precursor [Me 3 SbCH 2 COOH][Br] (2) and of [Me 3 SbCH 2 COOCH 2 CH 3 ][Br] (3) are reported. A new method for the synthesis of solvent‐free Me 3 Sb is described. The structures of 1·H 2 O and 3 were determined by single crystal X‐ray diffractometry. Copyright © 2002 John Wiley & Sons, Ltd.

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