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The synthesis of tetranuclear gold complexes, a structurally unprecedented octanuclear complex with a planar [Au I  8 ] core, and pentanuclear [Au I  4 M I ] (M=Cu, Ag) complexes is presented. The linear [Au I  4 ] complex undergoes C−H functionalization of carbonyl compounds under mild reaction conditions. In addition, [Au I  4 Ag I ] catalyzes the carbonylation of primary amines to form ureas under homogeneous conditions with efficiencies higher than those achieved by gold nanoparticles.

angewandte chemie international edition

Polynuclear Gold [Au I ] 4 , [Au I ] 8 , and Bimetallic [Au I  4 Ag I ] Complexes: C−H Functionalization of Carbonyl Compounds and Homogeneous Carbonylation of Amines