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SO(2) efficient : A three‐component palladium‐catalyzed coupling of aryl lithium compounds; sulfur dioxide (provided by the easy‐to‐handle solid surrogate, DABSO); and aryl, heteroaryl, and alkenyl (pseudo)halides yields a diverse library of sulfones. An electron‐poor XantPhos‐type ligand suppresses aryl–aryl exchange and is key to obtaining high yields.

Palladium‐Catalyzed Three‐Component Diaryl Sulfone Synthesis Exploiting the Sulfur Dioxide Surrogate DABSO