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Crosslinked Poly(ethylene oxide) as a Versatile Alignment Medium for the Measurement of Residual Anisotropic NMR Parameters
Author(s) -
Merle Christian,
Kummerlöwe Grit,
Freudenberger J. Christoph,
Halbach Felix,
Stöwer Wolfgang,
Gostomski Christoph Lierse v.,
Höpfner Johannes,
Beskers Timo,
Wilhelm Manfred,
Luy Burkhard
Publication year - 2013
Publication title -
angewandte chemie international edition
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 5.831
H-Index - 550
eISSN - 1521-3773
pISSN - 1433-7851
DOI - 10.1002/anie.201301929
Subject(s) - anisotropy , residual , ethylene oxide , oxide , solvent , poly ethylene , computer science , materials science , chemistry , ethylene , algorithm , physics , organic chemistry , polymer , optics , copolymer , catalysis
A universal alignment medium for the measurement of anisotropic NMR parameters that can be used for almost any type of sample would be highly useful for structure analysis in solution. Cross‐linked poly(ethylene oxide) with incredible solvent and solute compatibility range provides this medium. The picture shows residual 15 N chemical shift anisotropies (RCSAs) of 15 N‐labeled ubiquitin.