Orthorhombic In 2 O 3 : A Metastable Polymorph of Indium Sesquioxide | Zendy

Bekheet Maged F. | Zendy; Schwarz Marcus R. | Zendy; Lauterbach Stefan | Zendy; Kleebe HansJoachim | Zendy; Kroll Peter | Zendy; Riedel Ralf | Zendy; Gurlo Aleksander | Zendy

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Orthorhombic In 2 O 3 : A Metastable Polymorph of Indium Sesquioxide

Author(s) -

Bekheet Maged F.,

Schwarz Marcus R.,

Lauterbach Stefan,

Kleebe HansJoachim,

Kroll Peter,

Riedel Ralf,

Gurlo Aleksander

Publication year - 2013

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.201300644

Subject(s) - orthorhombic crystal system , sesquioxide , corundum , metastability , crystallography , indium , crystal structure , materials science , crystal (programming language) , chemistry , metallurgy , organic chemistry , computer science , programming language

The way is open for the physical and chemical characterization and single‐crystal growth of the orthorhombic o′‐In 2 O 3 polymorph. Orthorhombic In 2 O 3 is synthesized from rhombohedral corundum‐type rh‐In 2 O 3 under moderately high‐pressure and high‐temperature conditions (8–9 GPa, 600–1100 °C) followed by recovery to ambient pressure and temperature. The crystal‐structure data at ambient conditions confirm unambiguously the Rh 2 O 3 (II)‐type structure.

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