Pressure‐Induced Water Insertion in Synthetic Clays | Zendy

You Shujie | Zendy; Kunz Daniel | Zendy; Stöter Matthias | Zendy; Kalo Hussein | Zendy; Putz Bernd | Zendy; Breu Josef | Zendy; Talyzin Alexandr V. | Zendy

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Pressure‐Induced Water Insertion in Synthetic Clays

Author(s) -

You Shujie,

Kunz Daniel,

Stöter Matthias,

Kalo Hussein,

Putz Bernd,

Breu Josef,

Talyzin Alexandr V.

Publication year - 2013

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.201210060

Subject(s) - synchrotron , diamond anvil cell , phase transition , diffraction , materials science , layer (electronics) , phase (matter) , in situ , crystallography , chemistry , mineralogy , analytical chemistry (journal) , composite material , thermodynamics , optics , chromatography , organic chemistry , physics

A high‐pressure study of a synthetic smectite (Na‐fluorohectorite) immersed in liquid media was performed using in situ synchrotron X‐ray diffraction in a diamond anvil cell. A reversible phase transition because of the insertion of an additional water layer was observed for this material at 1.7 GPa. No similar transition was found when methanol was used as a pressure medium (see picture).

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