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Aiding the Self‐Assembly of Supramolecular Polyoxometalates under Hydrothermal Conditions To Give Precursors of Complex Functional Oxides
Author(s) -
Sanchez Sanchez Maricruz,
Girgsdies Frank,
Jastak Mateusz,
Kube Pierre,
Schlögl Robert,
Trunschke Annette
Publication year - 2012
Publication title -
angewandte chemie international edition
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 5.831
H-Index - 550
eISSN - 1521-3773
pISSN - 1433-7851
DOI - 10.1002/anie.201200746
Subject(s) - hydrothermal circulation , supramolecular chemistry , hydrothermal synthesis , computer science , nanotechnology , raman spectroscopy , chemistry , materials science , chemical engineering , molecule , physics , organic chemistry , engineering , optics
In situ Raman spectroscopy allows insight into molecular processes under hydrothermal conditions during synthesis of complex nanostructured MoVTeNb oxides (see picture: Nb yellow, Mo blue, V/Mo pale blue, Te red). Based on the knowledge acquired, the synthesis can be more efficiently directed towards the desired product with improved functionality.