Simple Determination of Double‐Bond Positions in Long‐Chain Olefins by Cross‐Metathesis | Zendy

Kwon Yongseok | Zendy; Lee Seonwoo | Zendy; Oh DongChan | Zendy; Kim Sanghee | Zendy

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Simple Determination of Double‐Bond Positions in Long‐Chain Olefins by Cross‐Metathesis

Author(s) -

Kwon Yongseok,

Lee Seonwoo,

Oh DongChan,

Kim Sanghee

Publication year - 2011

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.201102634

Subject(s) - derivatization , metathesis , double bond , simple (philosophy) , chemistry , olefin metathesis , salt metathesis reaction , mass spectrometry , combinatorial chemistry , computer science , chromatography , organic chemistry , polymerization , philosophy , epistemology , polymer

Cut, paste, and measure : The positions of double bonds in unsaturated long‐chain compounds can be easily determined by chemical derivatization using a cross‐metathesis reaction and chromatography–mass spectrometry. The produced olefins have distinct physicochemical properties suitable for LC/MS or GC/MS analysis that depend on the cross‐metathesis partner used. This method is operationally simple and applicable at a sub‐milligram scale.

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