A Selective Instant Synthesis of a Coordination Network and Its Ab Initio Powder Structure Determination | Zendy

Kawano Masaki | Zendy; Haneda Tsuyoshi | Zendy; Hashizume Daisuke | Zendy; Izumi Fujio | Zendy; Fujita Makoto | Zendy

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A Selective Instant Synthesis of a Coordination Network and Its Ab Initio Powder Structure Determination

Author(s) -

Kawano Masaki,

Haneda Tsuyoshi,

Hashizume Daisuke,

Izumi Fujio,

Fujita Makoto

Publication year - 2008

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.200704809

Subject(s) - ab initio , materials science , crystallization , powder diffraction , synchrotron , crystallography , diffraction , network structure , porosity , ab initio quantum chemistry methods , coordination number , crystal structure , instant , yield (engineering) , chemical engineering , molecule , chemistry , optics , organic chemistry , computer science , metallurgy , composite material , physics , ion , food science , engineering , machine learning

Fast powders and slow crystals : A uniform powder sample of a flexible porous coordination network is prepared in high yield by kinetically controlled synthesis and its crystal structure solved by synchrotron ab initio powder X‐ray diffraction (see picture). Crystals of a totally different porous network with larger channels for guest encapsulation are also obtained by thermodynamic control in a slow crystallization process.

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