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Multiple FID Acquisition of Complementary HMBC Data
Author(s) -
Nolis Pau,
PérezTrujillo Miriam,
Parella Teodor
Publication year - 2007
Publication title -
angewandte chemie international edition
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 5.831
H-Index - 550
eISSN - 1521-3773
pISSN - 1433-7851
DOI - 10.1002/anie.200702258
Subject(s) - content (measure theory) , abundance (ecology) , computer science , spectral line , data acquisition , information retrieval , chemistry , physics , mathematics , biology , mathematical analysis , astronomy , fishery , operating system
One experiment, four NMR spectra : By combining the principles of time‐sharing evolution and multiple FID acquisition within the same scan, several fully complementary NMR spectra can be obtained in a single‐shot acquisition. Four different HMBC and HMBC‐relayed experiments (see spectra) can be carried out simultaneously for 13 C and 15 N at natural abundance, with a saving in measuring time of up to 75 %.