One‐Pot Enzymatic Resolution and Separation of  sec ‐Alcohols Based on Ionic Acylating Agents | Zendy

Lourenço Nuno M. T. | Zendy; Afonso Carlos A. M. | Zendy

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One‐Pot Enzymatic Resolution and Separation of sec ‐Alcohols Based on Ionic Acylating Agents

Author(s) -

Lourenço Nuno M. T.,

Afonso Carlos A. M.

Publication year - 2007

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.200701774

Subject(s) - candida antarctica , ionic liquid , kinetic resolution , chemistry , resolution (logic) , acylation , lipase , transesterification , organic chemistry , enantiomer , solvent , extraction (chemistry) , chromatography , catalysis , enzyme , enantioselective synthesis , computer science , artificial intelligence

Going their different ways : A simple, robust, efficient, and reusable system for the one‐pot preparative resolution and separation of sec ‐alcohols is described. The system is based on the combination of sequential enzymatic kinetic resolution (lipase B from Candida Antarctica , CALB) and transesterification in ionic liquids (ILs) with an ionic acylating agent 1 and removal of each enantiomer by extraction with an organic solvent.

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