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Implementation of a Temperature‐Gradient Reactor System for High‐Throughput Investigation of Phosphonate‐Based Inorganic–Organic Hybrid Compounds
Author(s) -
Bauer Sebastian,
Stock Norbert
Publication year - 2007
Publication title -
angewandte chemie international edition
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 5.831
H-Index - 550
eISSN - 1521-3773
pISSN - 1433-7851
DOI - 10.1002/anie.200701575
Subject(s) - phosphonate , crystallization , phase diagram , throughput , phase (matter) , chemistry , chemical engineering , materials science , organic chemistry , computer science , telecommunications , engineering , wireless
Five new Cd phosphonates were discovered in a systematic investigation of the influence of the reaction temperature besides composition and pH value on the synthesis of inorganic–organic hybrid compounds in the CdCl 2 /H 5 L/NaOH system, which was achieved by the title procedure. In the resulting crystallization diagram (see picture), each color corresponds to a different phase.