Rapid Multiphase Carbonylation Reactions by Using a Microtube Reactor: Applications in Positron Emission Tomography  11 C‐Radiolabeling | Zendy

Miller Philip W. | Zendy; Long Nicholas J. | Zendy; de Mello Andrew J. | Zendy; Vilar Ramon | Zendy; Audrain Hélène | Zendy; Bender Dirk | Zendy; Passchier Jan | Zendy; Gee Antony | Zendy

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Rapid Multiphase Carbonylation Reactions by Using a Microtube Reactor: Applications in Positron Emission Tomography 11 C‐Radiolabeling

Author(s) -

Miller Philip W.,

Long Nicholas J.,

de Mello Andrew J.,

Vilar Ramon,

Audrain Hélène,

Bender Dirk,

Passchier Jan,

Gee Antony

Publication year - 2007

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.200604541

Subject(s) - carbonylation , carbon monoxide , palladium , catalysis , tube (container) , materials science , chemical reactor , chemistry , radiochemistry , chemical engineering , organic chemistry , composite material , engineering

Taking the tube : A silica‐supported palladium catalyst packed into teflon tubing is a simple, low‐cost, and effective method for carrying out carbonylative cross‐coupling reactions of arylhalides with amines and radiolabeled carbon monoxide gas. In carbonylation reactions, the microtube reactor displays enhanced yields over a short time period (12 min) compared with batch methods.

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