Glycosidation Promoted by a Reusable Solid Superacid in Supercritical Carbon Dioxide | Zendy

Li XueBing | Zendy; Ogawa Masato | Zendy; Monden Toshiki | Zendy; Maeda Takahiro | Zendy; Yamashita Eri | Zendy; Naka Mariko | Zendy; Matsuda Masao | Zendy; Hinou Hiroshi | Zendy; Nishimura ShinIchiro | Zendy

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Glycosidation Promoted by a Reusable Solid Superacid in Supercritical Carbon Dioxide

Author(s) -

Li XueBing,

Ogawa Masato,

Monden Toshiki,

Maeda Takahiro,

Yamashita Eri,

Naka Mariko,

Matsuda Masao,

Hinou Hiroshi,

Nishimura ShinIchiro

Publication year - 2006

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.200602161

Subject(s) - glycoconjugate , chemistry , supercritical fluid , reagent , supercritical carbon dioxide , organic chemistry , combinatorial chemistry , biochemistry

Superduper : A practical and cleaner synthetic protocol for various glycosides was established by means of a recyclable solid superacid promoter in supercritical carbon dioxide (scCO 2 ). Anomeric mixtures composed of α‐ and β‐isomers were successfully separated by employing supercritical fluid chromatography (SFC) with scCO 2 and methanol. L=leaving group, P=protecting group, ROH= sphingosine, sugar, etc.

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