Efficient Polymer‐Assisted Strategy for the Deprotection of Protected Oligosaccharides | Zendy

Tanaka Hiroshi | Zendy; Ishida Tadasuke | Zendy; Matoba Nobuatsu | Zendy; Tsukamoto Hirokazu | Zendy; Yamada Haruo | Zendy; Takahashi Takashi | Zendy

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Efficient Polymer‐Assisted Strategy for the Deprotection of Protected Oligosaccharides

Author(s) -

Tanaka Hiroshi,

Ishida Tadasuke,

Matoba Nobuatsu,

Tsukamoto Hirokazu,

Yamada Haruo,

Takahashi Takashi

Publication year - 2006

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.200601128

Subject(s) - trifluoroacetic acid , moiety , sugar , linker , chemistry , cleavage (geology) , protecting group , combinatorial chemistry , organic chemistry , computer science , biology , programming language , alkyl , fracture (geology) , paleontology

New strategies in sugar synthesis : A prelinker containing a dihydropyranyl moiety and an activated ester can be attached to a sugar, which is then loaded onto an amino‐modified support by amidation. Standard protecting‐group manipulations are possible. Final cleavage of the linker under mildly acidic conditions provides the fully deprotected oligosaccharides. TFA=trifluoroacetic acid.

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