Preparation, Characterization, and Crystal Structures of the SO 3 NHF −  and SO 3 NF 2  −  Ions | Zendy

Haiges Ralf | Zendy; Wagner Ross | Zendy; Boatz Jerry A. | Zendy; Yousufuddin Muhammed | Zendy; Etzkorn Markus | Zendy; Prakash G. K. Surya | Zendy; Christe Karl O. | Zendy; Chapman Robert D. | Zendy; Welker Mark F. | Zendy; Kreutzberger Charles B. | Zendy

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Preparation, Characterization, and Crystal Structures of the SO 3 NHF − and SO 3 NF 2 − Ions

Author(s) -

Haiges Ralf,

Wagner Ross,

Boatz Jerry A.,

Yousufuddin Muhammed,

Etzkorn Markus,

Prakash G. K. Surya,

Christe Karl O.,

Chapman Robert D.,

Welker Mark F.,

Kreutzberger Charles B.

Publication year - 2006

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.200601020

Subject(s) - reagent , ion , characterization (materials science) , aqueous solution , chemistry , inorganic chemistry , crystal (programming language) , radiochemistry , crystallography , nuclear chemistry , materials science , nanotechnology , organic chemistry , computer science , programming language

Safe difluoroaminating reagents : Salts of the elusive SO 3 NF 2 − ion were prepared by aqueous fluorination of SO 3 NH 2 − with F 2 . These salts were characterized (see ORTEP of the anion) and shown to be excellent reagents for the preparation of gem ‐bis(difluoroamines). Salts of the intermediate SO 3 NHF − ion were also isolated and characterized.

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