Room‐Temperature Swern Oxidations by Using a Microscale Flow System | Zendy

Kawaguchi Tatsuya | Zendy; Miyata Hiroyuki | Zendy; Ataka Kikuo | Zendy; Mae Kazuhiro | Zendy; Yoshida Junichi | Zendy

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Room‐Temperature Swern Oxidations by Using a Microscale Flow System

Author(s) -

Kawaguchi Tatsuya,

Miyata Hiroyuki,

Ataka Kikuo,

Mae Kazuhiro,

Yoshida Junichi

Publication year - 2005

Publication title -

angewandte chemie international edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 1433-7851

DOI - 10.1002/anie.200462466

Subject(s) - swern oxidation , microreactor , microscale chemistry , flow chemistry , chemistry , trifluoroacetic anhydride , exothermic reaction , organic synthesis , organosulfur compounds , organic chemistry , chemical engineering , dimethyl sulfoxide , catalysis , sulfur , mathematics education , mathematics , engineering

Residence time controlled reaction : The Swern oxidation of alcohols has been accomplished by using a microscale flow system, consisting of micromixers and microscale tube reactors (see schematic representation; DMSO=dimethylsulfoxide, TFAA=trifluoroacetic anhydride), at higher temperatures (−20 to 20 °C) than those for conventional macroscale batch systems (−50 °C or below).

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