Isolation and X‐ray Crystallographic Analysis of a Stable Selenenic Acid | Zendy

Saiki Toshiyuki | Zendy; Goto Kei | Zendy; Okazaki Renji | Zendy

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Isolation and X‐ray Crystallographic Analysis of a Stable Selenenic Acid

Author(s) -

Saiki Toshiyuki,

Goto Kei,

Okazaki Renji

Publication year - 1997

Publication title -

angewandte chemie international edition in english

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 0570-0833

DOI - 10.1002/anie.199722231

Subject(s) - steric effects , electromagnetic shielding , decomposition , isolation (microbiology) , chemistry , crystallography , group (periodic table) , materials science , stereochemistry , organic chemistry , bioinformatics , biology , composite material

The deep cavity in the calix[6]arene framework provides a sterically shielded environment for the SeOH group of the selenenic acid 1 . Thanks to this shielding the compound is extraordinarily stable—no decomposition was observed even after heating at 120°C for 5 h in CDCl 2 CDCl 2 —although the functional group is still reactive.

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