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Molecular Structure of [Pd 6 Cl 12 ] in Single Crystals Chemically Grown at Room Temperature
Author(s) -
Dell'Amico Daniela Belli,
Calderazzo Fausto,
Marchetti Fabio,
Ramello Stefano
Publication year - 1996
Publication title -
angewandte chemie international edition in english
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 5.831
H-Index - 550
eISSN - 1521-3773
pISSN - 0570-0833
DOI - 10.1002/anie.199613311
Subject(s) - thionyl chloride , single crystal , diffraction , chloride , chemistry , x ray crystallography , characterization (materials science) , crystallography , partial pressure , powder diffraction , crystal structure , inorganic chemistry , analytical chemistry (journal) , materials science , organic chemistry , nanotechnology , optics , physics , oxygen
A reduction of the CO partial pressure is sufficient to obtain single crystals of [Pd 6 Cl 12 ] from the equilibrium (a) in thionyl chloride (solv.) at room temperature. The single‐crystal and powder X‐ray diffraction characterization of this Pd II chloride is described.