Formation of a Porous Zirconium Oxo Phosphate with a High Surface Area by a Surfactant‐Assisted Synthesis | Zendy

Ciesla Ulrike | Zendy; Schacht Stefan | Zendy; Stucky Galen D. | Zendy; Unger Klaus K. | Zendy; Schüth Ferdi | Zendy

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Formation of a Porous Zirconium Oxo Phosphate with a High Surface Area by a Surfactant‐Assisted Synthesis

Author(s) -

Ciesla Ulrike,

Schacht Stefan,

Stucky Galen D.,

Unger Klaus K.,

Schüth Ferdi

Publication year - 1996

Publication title -

angewandte chemie international edition in english

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 0570-0833

DOI - 10.1002/anie.199605411

Subject(s) - zirconium , phosphoric acid , pulmonary surfactant , calcination , aqueous solution , sulfate , phosphate , zirconium phosphate , porosity , inorganic chemistry , bet theory , specific surface area , materials science , chemistry , chemical engineering , adsorption , organic chemistry , catalysis , engineering , biochemistry

Analogous to the synthesis of MCM‐41 , a mesostructured product (shown schematically on the right) can be obtained from aqueous solutions of zirconium sulfate by addition of alkyltrimethylammonium salts. After a treatment with phosphoric acid, this material can be calcined without structural collapse. The resulting zirconium oxo phosphate shows BET surface areas of up to 400 m 2 g −1 .

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