A Reagent for Determining Optical Purities of Diols by Formation of Diastereomeric Arylboronate Esters | Zendy

Burgess Kevin | Zendy; Porte Alexander M. | Zendy

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A Reagent for Determining Optical Purities of Diols by Formation of Diastereomeric Arylboronate Esters

Author(s) -

Burgess Kevin,

Porte Alexander M.

Publication year - 1994

Publication title -

angewandte chemie international edition in english

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 0570-0833

DOI - 10.1002/anie.199411821

Subject(s) - diastereomer , reagent , derivatization , enantioselective synthesis , chemistry , diol , organic chemistry , combinatorial chemistry , chromatography , high performance liquid chromatography , catalysis

A remarkably simple arylboronic acid reagent for derivatization of diols enables the determination of the optical purity of diols by 1 H NMR spectroscopy by the formation of the corresponding esters 1 . This procedure could be particularly valuable as enantioselective bishydroxylations become more widely used for asymmetric syntheses.

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