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FAST NOESY Experiments—An Approach for Fast Structure Determination
Author(s) -
Köck Matthias,
Griesinger Christian
Publication year - 1994
Publication title -
angewandte chemie international edition in english
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 5.831
H-Index - 550
eISSN - 1521-3773
pISSN - 0570-0833
DOI - 10.1002/anie.199403321
Subject(s) - two dimensional nuclear magnetic resonance spectroscopy , spectral line , nuclear overhauser effect , relaxation (psychology) , reliability (semiconductor) , chemistry , nuclear magnetic resonance , physics , nuclear magnetic resonance spectroscopy , biology , quantum mechanics , power (physics) , neuroscience
NOESY spectra can be acquired five to ten times faster with the procedure described here. The reliability of the internuclear distances obtained from these spectra does not suffer. In addition to recording the FAST NOESY spectra, only the relaxation times T 1 of the protons must be determined.