Synthesis of the Mono(Dewar Benzene) Isomer of [1.1]Metacyclophane | Zendy

Wijsman Geerlig W. | Zendy; van Es Daniël S. | Zendy; de Wolf Willem H. | Zendy; Bickelhaupt Friedrich | Zendy

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Synthesis of the Mono(Dewar Benzene) Isomer of [1.1]Metacyclophane

Author(s) -

Wijsman Geerlig W.,

van Es Daniël S.,

de Wolf Willem H.,

Bickelhaupt Friedrich

Publication year - 1993

Publication title -

angewandte chemie international edition in english

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 0570-0833

DOI - 10.1002/anie.199307261

Subject(s) - benzene , chemistry , mass spectrometry , derivative (finance) , high resolution , nuclear magnetic resonance spectroscopy , stereochemistry , organic chemistry , chromatography , geology , financial economics , economics , remote sensing

An unsaturated, highly strained [5]metacyclophane derivative is one description of compound 2 , which was obtained by the reaction of the hexahalobispropellane precursor 1 (X C1) with t BuOK in dimethylsulfoxide. Compound 2 was characterized by NMR spectroscopy and high‐resolution mass spectrometry.

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