A Telluradistannirane and a 1,3‐Ditelluradistannetane by Stepwise Addition of Tellurium to a Distannene | Zendy

Schäfer Annemarie | Zendy; Weidenbruch Manfred | Zendy; Saak Wolfgang | Zendy; Pohl Siegfried | Zendy; Marsmann Heinrich | Zendy

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A Telluradistannirane and a 1,3‐Ditelluradistannetane by Stepwise Addition of Tellurium to a Distannene

Author(s) -

Schäfer Annemarie,

Weidenbruch Manfred,

Saak Wolfgang,

Pohl Siegfried,

Marsmann Heinrich

Publication year - 1991

Publication title -

angewandte chemie international edition in english

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 0570-0833

DOI - 10.1002/anie.199108341

Subject(s) - tellurium , aryl , reagent , yield (engineering) , tin , chemistry , ring (chemistry) , thermal decomposition , medicinal chemistry , combinatorial chemistry , organic chemistry , materials science , alkyl , metallurgy

A reactive SnSn multiple bond system is found in distannane 1 , as evidenced by the smooth reaction with tellurium to form the Sn 2 Te three‐membered ring 2 . Compound 1 is formed by thermolysis of the corresponding substituted cyclotristannane, which is prepared by a surprisingly simple, high‐yield synthesis from an aryl Grignard reagent with tin(II) chloride. Aryl = 2,4,6‐ i Pr 3 C 6 H 2 .

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