Gas Chromatographic Determination of the Enantiomeric Composition of Epoxy Alcohols | Zendy

König Wilfried A. | Zendy; Lutz Sabine | Zendy; Wenz Gerhard | Zendy; Görgen Günther | Zendy; Neumann Christoph | Zendy; Gäbler Andreas | Zendy; Boland Wilhelm | Zendy

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Gas Chromatographic Determination of the Enantiomeric Composition of Epoxy Alcohols

Author(s) -

König Wilfried A.,

Lutz Sabine,

Wenz Gerhard,

Görgen Günther,

Neumann Christoph,

Gäbler Andreas,

Boland Wilhelm

Publication year - 1989

Publication title -

angewandte chemie international edition in english

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 0570-0833

DOI - 10.1002/anie.198901781

Subject(s) - epoxy , enantiomer , chemistry , chromatography , capillary gas chromatography , gas chromatography , composition (language) , organic chemistry , linguistics , philosophy

Enantiomeric excesses greater than 98% can now be determined exactly in the synthesis of chiral epoxy alcohols. Capillary chromatography on peralkylated cyclodextrins allows the trifluoroacetyl derivatives of epoxy alcohols such as ( E )‐2,3‐epoxy‐4‐octynol (picture on the right) and 2,3‐epoxypropanol to be separated into their enantiomers within a few minutes.

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