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A Stable 1,2,4‐Thiadiphosphole (“2,4‐Diphosphathiophene”)
Author(s) -
Appel Rolf,
Moors Rainer
Publication year - 1986
Publication title -
angewandte chemie international edition in english
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 5.831
H-Index - 550
eISSN - 1521-3773
pISSN - 0570-0833
DOI - 10.1002/anie.198605671
Subject(s) - mass spectrometry , sequence (biology) , nuclear magnetic resonance spectroscopy , chemistry , spectroscopy , stereochemistry , chromatography , physics , biochemistry , quantum mechanics
The new C 2 P 2 S heterocycle 1 with a PCPC sequence was obtained from CS 2 , LiP(SiMe 3 ) 2 , and Me 3 SiCl. The structure of the yellow, distillable liquid was determined by 31 P‐, 13 C‐, and 29 Si‐NMR spectroscopy and by mass spectrometry.