Dilithio(phenylsulfonyl)trimethylsilylmethane: Synthesis, 13C/1H‐NMR Characterization, and Lithium‐Titanium Exchange | Zendy

Vollhardt Jürgen | Zendy; Gais HansJoachim | Zendy; Lukas Karl L. | Zendy

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Dilithio(phenylsulfonyl)trimethylsilylmethane: Synthesis, 13C/1H‐NMR Characterization, and Lithium‐Titanium Exchange

Author(s) -

Vollhardt Jürgen,

Gais HansJoachim,

Lukas Karl L.

Publication year - 1985

Publication title -

angewandte chemie international edition in english

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 5.831

H-Index - 550

eISSN - 1521-3773

pISSN - 0570-0833

DOI - 10.1002/anie.198506961

Subject(s) - sulfone , lithium (medication) , trimethylsilyl , titanium , chemistry , carbon 13 nmr , characterization (materials science) , organic chemistry , materials science , nanotechnology , medicine , endocrinology

The first dilithioalkyl sulfone, the title compound 2, was obtained by stepwise lithiation of the trimethylsilyl sulfone 1 with nBuLi. Compounds such as 2 are of interst with respect to their structure and their synthetic potential, e.g., for the preparation of novel functionalized organometallic compounds.

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