Palladium‐Catalyzed Cross‐Coupling/Annulation Cascade for Synthesis of 9‐Hydroxy and 9‐Aminofluorenes. | Zendy

François Benjamin | Zendy; Szczubelek Luc | Zendy; Berrée Fabienne | Zendy; Roisnel Thierry | Zendy; Carboni Bertrand | Zendy

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Palladium‐Catalyzed Cross‐Coupling/Annulation Cascade for Synthesis of 9‐Hydroxy and 9‐Aminofluorenes.

Author(s) -

François Benjamin,

Szczubelek Luc,

Berrée Fabienne,

Roisnel Thierry,

Carboni Bertrand

Publication year - 2018

Publication title -

advanced synthesis and catalysis

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.541

H-Index - 155

eISSN - 1615-4169

pISSN - 1615-4150

DOI - 10.1002/adsc.201701146

Subject(s) - annulation , palladium , intermolecular force , tandem , catalysis , cascade , chemistry , hydrogen bond , sequence (biology) , coupling (piping) , cascade reaction , combinatorial chemistry , stereochemistry , organic chemistry , molecule , materials science , biochemistry , chromatography , composite material , metallurgy

9‐Hydroxyfluorenes are easily synthesized via a tandem Suzuki/phenolic aldolisation sequence. This process was extended to 9‐aminofluorenes by simply adding various amines as third partners. X‐ray structures and NMR studies confirmed the presence of intermolecular O−H ⋅ ⋅ ⋅ N hydrogen bonding.

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