Iron‐Catalyzed C( sp  3 )−C( sp  3 ) Bond Formation in 3,4‐Dihydro‐1,4‐benzoxazin‐2‐ones | Zendy

Dong Jie | Zendy; Min Wenjian | Zendy; Li Haitao | Zendy; Quan Zhengjun | Zendy; Yang Caixia | Zendy; Huo Congde | Zendy

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Iron‐Catalyzed C( sp 3 )−C( sp 3 ) Bond Formation in 3,4‐Dihydro‐1,4‐benzoxazin‐2‐ones

Author(s) -

Dong Jie,

Min Wenjian,

Li Haitao,

Quan Zhengjun,

Yang Caixia,

Huo Congde

Publication year - 2017

Publication title -

advanced synthesis and catalysis

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.541

H-Index - 155

eISSN - 1615-4169

pISSN - 1615-4150

DOI - 10.1002/adsc.201700816

Subject(s) - chemistry , catalysis , alkyl , medicinal chemistry , transformation (genetics) , coupling reaction , organic chemistry , biochemistry , gene

A convenient iron‐catalyzed oxidative dehydrogenative coupling reaction of 3,4‐Dihydro‐1,4‐benzoxazin‐2‐ones with malonic esters or ketones was performed under mild reaction conditions to construct alkyl–alkyl C( sp 3 )−C( sp 3 ) bonds. This transformation can be catalyzed efficiently by magnetically recoverable iron nanoparticles and the catalyst can be recycled easily for 7 times without decreasing activity.

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