Suzuki–Miyaura Cross‐Coupling under Solvent‐Free Conditions | Zendy

Asachenko Andrey F. | Zendy; Sorochkina Kristina R. | Zendy; Dzhevakov Pavel B. | Zendy; Topchiy Maxim A. | Zendy; Nechaev Mikhail S. | Zendy

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Suzuki–Miyaura Cross‐Coupling under Solvent‐Free Conditions

Author(s) -

Asachenko Andrey F.,

Sorochkina Kristina R.,

Dzhevakov Pavel B.,

Topchiy Maxim A.,

Nechaev Mikhail S.

Publication year - 2013

Publication title -

advanced synthesis and catalysis

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.541

H-Index - 155

eISSN - 1615-4169

pISSN - 1615-4150

DOI - 10.1002/adsc.201300741

Subject(s) - chemistry , palladium , aryl , triphenylphosphine , pinacol , solvent , catalysis , coupling reaction , suzuki reaction , halide , chloride , organic chemistry , medicinal chemistry , alkyl

A solvent‐free reaction protocol for Suzuki–Miyaura cross‐couplings was developed. (Hetero)aryl bromides and chlorides are coupled with pinacol arylboronates in high yields. The reaction is catalyzed by conventional bis(triphenylphosphine)palladium(II) chloride [(PPh 3 ) 2 PdCl 2 ] and/or palladium(II) acetate/SPhos [Pd(OAc) 2 /SPhos] under air.

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