Batch Stille Coupling with Insoluble and Recyclable Stannylated Polynorbornenes | Zendy

MartínezArranz Sheila | Zendy; Carrera Nora | Zendy; Albéniz Ana C. | Zendy; Espinet Pablo | Zendy; VidalMoya Alejandro | Zendy

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Batch Stille Coupling with Insoluble and Recyclable Stannylated Polynorbornenes

Author(s) -

MartínezArranz Sheila,

Carrera Nora,

Albéniz Ana C.,

Espinet Pablo,

VidalMoya Alejandro

Publication year - 2012

Publication title -

advanced synthesis and catalysis

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.541

H-Index - 155

eISSN - 1615-4169

pISSN - 1615-4150

DOI - 10.1002/adsc.201200624

Subject(s) - stille reaction , reagent , chemistry , tin , coupling (piping) , polymer , organic chemistry , polymer chemistry , combinatorial chemistry , composite material , materials science

The Stille coupling can be carried out in a batch process using insoluble tin supports. The new type of support consists of stannylated polymers based on the vinylic polynorbornene skeleton that allow one to use a set‐up where the tin reagent is immobilized in a column. The immobilized stannylated polymeric reagent can be easily reused. The coupling products are thus obtained by a very simple work‐up procedure and have very low levels of tin contamination.

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