Ligand‐Free and Heterogeneous Palladium on Carbon‐Catalyzed Hetero‐Suzuki–Miyaura Cross‐Coupling | Zendy

Kitamura Yoshiaki | Zendy; Sako Satoko | Zendy; Tsutsui Azusa | Zendy; Monguchi Yasunari | Zendy; Maegawa Tomohiro | Zendy; Kitade Yukio | Zendy; Sajiki Hironao | Zendy

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Ligand‐Free and Heterogeneous Palladium on Carbon‐Catalyzed Hetero‐Suzuki–Miyaura Cross‐Coupling

Author(s) -

Kitamura Yoshiaki,

Sako Satoko,

Tsutsui Azusa,

Monguchi Yasunari,

Maegawa Tomohiro,

Kitade Yukio,

Sajiki Hironao

Publication year - 2010

Publication title -

advanced synthesis and catalysis

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.541

H-Index - 155

eISSN - 1615-4169

pISSN - 1615-4150

DOI - 10.1002/adsc.200900638

Subject(s) - chemistry , palladium , alicyclic compound , ligand (biochemistry) , catalysis , coupling reaction , suzuki reaction , carbon fibers , combinatorial chemistry , organic chemistry , polymer chemistry , biochemistry , materials science , receptor , composite number , composite material

A ligand‐free and heterogeneous palladium on carbon (Pd/C)‐catalyzed hetero‐Suzuki–Miyaura coupling reaction has been developed. The protocol enables the construction of both heterocyclic‐alicyclic and heterocyclic‐heterocyclic biaryl derivatives in good to excellent yields. Furthermore, Pd/C could be reused. The time‐course study clarified that palladium was leached into the reaction media as the reaction proceeded and then completely deposited on the carbon support.

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