Purification of Fluorous Mitsunobu Reactions by Liquid‐Liquid Extraction | Zendy

Curran Dennis P. | Zendy; Bajpai Reena | Zendy; Sanger Elizabeth | Zendy

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Purification of Fluorous Mitsunobu Reactions by Liquid‐Liquid Extraction

Author(s) -

Curran Dennis P.,

Bajpai Reena,

Sanger Elizabeth

Publication year - 2006

Publication title -

advanced synthesis and catalysis

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.541

H-Index - 155

eISSN - 1615-4169

pISSN - 1615-4150

DOI - 10.1002/adsc.200606187

Subject(s) - chemistry , reagent , partition coefficient , mitsunobu reaction , solvent , organic solvent , liquid–liquid extraction , extraction (chemistry) , chromatography , solvent extraction , organic chemistry , combinatorial chemistry , chemical engineering , engineering

Solvent tuning and partition coefficient measurements have identified suitable reagent and solvent combinations for the purification of fluorous Mitsunobu reaction products. The crude reaction mixtures are partitioned between 2/1 HFE‐7100/FC‐72 and DMF/10 % water to provide reagent (fluorous) and product (organic) fractions.

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