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High‐Pressure Multianvil Synthesis and Structure Refinement of Oxygen‐Bearing Cubic Zirconium(IV) Nitride
Author(s) -
Dzivenko D. A.,
Zerr A.,
Bulatov V. K.,
Miehe G.,
Li J.,
Thybusch B.,
Brötz J.,
Fueß H.,
Brey G.,
Riedel R.
Publication year - 2007
Publication title -
advanced materials
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 10.707
H-Index - 527
eISSN - 1521-4095
pISSN - 0935-9648
DOI - 10.1002/adma.200602610
Subject(s) - materials science , zirconium nitride , zirconium , raman spectroscopy , nitride , diffraction , oxygen , crystallography , high pressure , crystal structure , bearing (navigation) , metallurgy , composite material , thermodynamics , layer (electronics) , organic chemistry , optics , titanium nitride , chemistry , physics , cartography , geography
Macroscopic amounts of oxygen‐bearing c‐Zr 3 N 4 with a cubic Th 3 P 4 ‐type structure are synthesized for the first time (see figure) at high pressures and temperatures. Structure refinement based on X‐ray diffraction data is performed. The Raman spectrum, morphology, and microhardness of the synthesized material is measured.