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Microstructural Parameters and Their Effect on the Indentation Hardness of Electrodeposited and Annealed Nickel–Iron Micro‐Specimens
Author(s) -
Schmitt MartinT.,
Hoffmann Joachim E.,
Eifler Dietmar
Publication year - 2013
Publication title -
advanced engineering materials
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.938
H-Index - 114
eISSN - 1527-2648
pISSN - 1438-1656
DOI - 10.1002/adem.201200253
Subject(s) - materials science , microstructure , grain size , annealing (glass) , indentation , metallurgy , transmission electron microscopy , nickel , indentation hardness , atmospheric temperature range , composite material , scanning electron microscope , liga , grain growth , fabrication , nanotechnology , meteorology , medicine , physics , alternative medicine , pathology
Using the direct‐LIGA technology, nickel–iron micro‐specimens are serially produced by a micro‐gear drive manufacturer and subsequently annealed within the temperature range between 180 and 800 °C. The microstructure (grain size, lattice strain, and texture) is characterized using XRD measurements. Following electrodeposition, nano‐crystalline microstructures result with grain size of approximately 10 nm. The transmission electron microscope images confirm the XRD results. The lattice strain decreases in the temperature range from 200 to 300 °C and grain growth results for an annealing temperature from approximately 260 °C. The annealing treatment produced no essential changes in the material's texture. Analysis of the indentation hardness and indentation modulus demonstrates considerable changes above 200 °C.