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Recent Advances in High‐Resolution Solid‐State NMR Spectroscopy
Author(s) -
Schwalbe Harald,
Bielecki Anthony
Publication year - 2001
Publication title -
angewandte chemie international edition
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 5.831
H-Index - 550
eISSN - 1521-3773
pISSN - 1433-7851
DOI - 10.1002/1521-3773(20010601)40:11<2045::aid-anie2045>3.0.co;2-s
Subject(s) - solid state nuclear magnetic resonance , magic angle spinning , spectroscopy , nuclear magnetic resonance spectroscopy , high resolution , solid state , magic angle , materials science , spinning , chemistry , crystallography , chemical physics , nuclear magnetic resonance , physics , stereochemistry , polymer chemistry , remote sensing , quantum mechanics , geology
Diverse complex systems may be studied by the new methods in solid‐state NMR spectroscopy described herein. These methods use magic‐angle spinning (MAS) on samples in oriented bilayers (right picture) and in orientationally disordered samples (left picture). Systems as diverse as uniformly 13 C, 15 N‐labeled proteins, model membrane systems, and silk, as produced by the silkworm, can be structurally characterized.