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Separation of D ‐lysergic acid diethylamide derivatives using micellar electrokinetic capillary chromatography
Author(s) -
Djordjevic M. Nebojsa,
Fitzpatrick Fiona,
Houdiere Fabrice
Publication year - 2000
Publication title -
electrophoresis
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.666
H-Index - 158
eISSN - 1522-2683
pISSN - 0173-0835
DOI - 10.1002/(sici)1522-2683(20000301)21:4<724::aid-elps724>3.0.co;2-5
Subject(s) - micellar electrokinetic chromatography , electrokinetic phenomena , chromatography , chemistry , lysergic acid diethylamide , electric field , lysergic acid , capillary action , analytical chemistry (journal) , micelle , capillary electrophoresis , materials science , organic chemistry , biochemistry , physics , receptor , aqueous solution , quantum mechanics , serotonin , composite material
By adjusting column temperature and applied electric field, a fast separation in micellar electrokinetic capillary chromatography was developed for the separation of D ‐lysergic acid diethylamide derivatives. A baseline separation of nine derivatives was accomplished with a run time of less than 12 min by utilizing elevated column temperature (60°C) and an applied electric field of 387 V/cm. The number of plates generated per unit time for the separations completed at elevated temperatures was significantly higher when compared to separations at the same applied electric field but at lower temperatures (20°C).