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A Parametric Study of the Synthesis of 4,4′,5,5′,7,7′‐Hexanitro‐1,1′‐Binaphthyl
Author(s) -
Duffin Henry C.,
Golding Peter,
Wells Clifford H. J.
Publication year - 1998
Publication title -
propellants, explosives, pyrotechnics
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.56
H-Index - 65
eISSN - 1521-4087
pISSN - 0721-3115
DOI - 10.1002/(sici)1521-4087(199811)<244::aid-prep244>3.0.co;2-7
Subject(s) - nitration , yield (engineering) , chemistry , physics , organic chemistry , thermodynamics
Conditions for the synthesis of 4,4′,5,5′,7,7′‐hexanitrobinaphthyl( I ) from 1,1′‐binaphthyl have been investigated. It has been found that( I ) can be prepared in 50% yield in a two‐stage nitration process.