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Synthesis of 2S,4′R,8′R‐α‐[5‐methyl‐ 14 C]tocopheryl acetate
Author(s) -
Nakamura T.,
Hamamura K.,
Ueda T.
Publication year - 2000
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/(sici)1099-1344(200002)43:2<185::aid-jlcr310>3.0.co;2-9
Subject(s) - chemistry , tocopheryl acetate , phytol , enantiomer , chromatography , high performance liquid chromatography , organic chemistry , stereochemistry , biochemistry , vitamin e , antioxidant
2‐Ambo‐γ‐tocopheryl acetate 4 was synthesized starting from 2,3‐dimethylhydroquinone monobenzoate 1 and natural phytol 2 . 2S,4′R,8′R‐enantiomer 6 was separated using preparative Chiralpack OP (+) column HPLC. Copyright © 2000 John Wiley & Sons, Ltd.