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Synthesis of 3 H‐SCH 51048 and 14 C‐SCH 56592
Author(s) -
Magatti C. V.,
Hesk D.,
Lauzon M. J.,
Saluja S. S.,
Wang X.
Publication year - 1998
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/(sici)1099-1344(1998080)41:8<731::aid-jlcr125>3.0.co;2-t
Subject(s) - chemistry , yield (engineering) , tritium , specific activity , radiochemistry , catalysis , carbon 14 , nuclear chemistry , organic chemistry , enzyme , nuclear physics , physics , materials science , metallurgy
3 H‐SCH 51048 and 14 C‐SCH 56592 have been synthesized. 3 H‐SCH 51048 was prepared in two steps by acid catalyzed tritium exchange while 14 C‐SCH 56592 was prepared in three steps from 14 C‐formamidine acetate in an overall 21% radiochemical yield. © 1998 John Wiley & Sons, Ltd.