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Efficient syntheses of multiply 2 H‐ and 13 C‐labeled acrylic acid, glyceric acid, glycidic acid and glycerol
Author(s) -
Pitlik János,
Townsend Craig A.
Publication year - 1997
Publication title -
journal of labelled compounds and radiopharmaceuticals
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.432
H-Index - 47
eISSN - 1099-1344
pISSN - 0362-4803
DOI - 10.1002/(sici)1099-1344(199712)39:12<999::aid-jlcr45>3.0.co;2-q
Subject(s) - glyceric acid , chemistry , glycerol , acrylate , acrylic acid , organic chemistry , copolymer , polymer
Syntheses of multiply 2 H‐ and 13 C‐labeled C‐3 carbohydrates have been carried out from commercially available [1,2‐ 13 C 2 ]bromoacetic acid. The syntheses are illustrated for [1,2‐ 13 C 2 ]acrylate, [2,3,3‐ 2 H 3 , 1,2‐ 13 C 2 ]acrylate, [1,2‐ 13 C 2 ]glycerate, [2,3,3‐ 2 H 3 , 1,2‐ 13 C 2 ]glycerate, [1,2‐ 13 C 2 ]glycidate and [1,1‐ 2 H 2 , 1,2‐ 13 C 2 ]glycerol. © 1997 John Wiley & Sons, Ltd.