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Specific Isotope Enrichment of Methyl Methacrylate
Author(s) -
Werkhoven Thekla M.,
van Nispen Reinier,
Lugtenburg Johan
Publication year - 1999
Publication title -
european journal of organic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.825
H-Index - 155
eISSN - 1099-0690
pISSN - 1434-193X
DOI - 10.1002/(sici)1099-0690(199911)1999:11<2909::aid-ejoc2909>3.0.co;2-5
Subject(s) - chemistry , methyl methacrylate , methacrylate , isotope , poly(methyl methacrylate) , combinatorial chemistry , organic chemistry , polymerization , polymer , physics , quantum mechanics
A synthetic scheme has been developed to prepare methyl methacrylate specifically 13 C‐labelled at all different positions and in any combination of positions, from simple, commercially available starting materials. According to this scheme methyl (1‐ 13 C)‐ and methyl (2‐ 13 C)methacrylate ( 1a and 1b ) have been prepared with high label incorporation (99%).